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Green Analytical Chemistry
Scopus
ISSN 2772-5774 · Elsevier · 349 artikel di indeks
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Artikel Jurnal
A sustainable analytical workflow for microplastic detection and typification via NIR-HSI: Validation through sea salt analysis
This work presents a sustainable analytical workflow for the detection and typification of microplastics (MPs) in environmental matrices using Near Infrared Hyperspectral Imaging (NIR-HSI) combined with chemometrics. The proposed methodology enables rapid, non-destructive, and solvent-free…
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Artikel Jurnal
Green ultrasound-assisted extraction and GC-MS for the identification of intentionally and non-intentionally added substances in bio-based food contact materials
The use of bioplastics as food contact materials (FCMs) is rapidly expanding as a sustainable alternative to conventional plastics, with polylactic acid (PLA) being among the most widely used biopolymer. The complex nature of bioplastics makes extraction and detection of intentionally and…
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Artikel Jurnal
QSPR-driven prediction of analyte permeability for advancing CP-MIMS applications
Condensed Phase-Membrane Introduction Mass Spectrometry (CP-MIMS) is a sustainable and highly versatile approach within the framework of Direct Mass Spectrometry techniques, which enables real-time determination of target analytes by integrating sampling, purification, and mass-spectrometric…
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Artikel Jurnal
Reliable spectroscopic screening protocols for the eco-design of analytical workflows in laboratories ensuring EVOO quality categorisation
The increasing demand for food safety/quality and environmental sustainability requires the development of rapid, reliable and green analytical screening methods for food quality assessment. Although precise, traditional reference methods are often time-consuming, resource-intensive and…
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Artikel Jurnal
Towards circular analytical chemistry: Optimization of colorimetric assay for sustainable and selective dopamine detection in pharmaceutical formulations using green solvents
The drive towards sustainability in analytical chemistry has prompted the replacement of hazardous solvents with greener alternatives, in line with circular chemistry principles. We here report a rapid, low-cost, and sustainable colorimetric assay for dopamine (DA) detection in pharmaceutical…
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Artikel Jurnal
AI-assisted design and optimization of two smart green HPLC methods for simultaneous determination of some antiviral drugs
Two novel high-performance liquid chromatography (HPLC) methods were developed and validated for the determination of dolutegravir (DTG), lamivudine (3TC), and abacavir (ABA) in pharmaceutical formulations. In this study, AI engines such as Copilot, ChatGPT 5.2, Gemini, and Perplexity were…
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Artikel Jurnal
Comprehensive metric-based assessment of fabric phase sorptive extraction’s greenness and operational performance in water sample preparation and analysis
Fabric phase sorptive extraction (FPSE) is a sample preparation technique that has gained significant attention due to its operational simplicity, low solvent consumption, and improved sorbent loading relative to traditional extraction techniques. In this study, the greenness and practicality of…
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Artikel Jurnal
Quantitative structure retention relationship applied to capillary scale liquid chromatography for the identification of phenolic compounds
Quantitative Structure-Retention Relationship (QSRR) model was developed to predict retention data of phenolic compounds and elucidate their retention mechanisms under reversed phase conditions. Compared to a previous work (Laganà-Vinci et al., J. Chromatogr. A, 2024, 1730, 465,146), the…
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Artikel Jurnal
Development and validation of quality by design guided HPTLC method for estimation of β-sitosterol in Celastrus paniculatus seed oil and its nano-formulation with greenness evaluation
Background: Celastrus paniculatus is an ethnomedicinally important shrub, belonging to the Celastraceae family. Its seed oil demonstrates diverse pharmacological activities. However, no Quality by Design (QbD)-based analytical method has been reported to date to estimate of β-sitosterol in…
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Artikel Jurnal
Nanotechnology in environmental remediation: Transforming pollution control across diverse matrices
Environmental pollution, encompassing water contamination, air degradation, and microplastic proliferation, poses significant threats to ecosystems and human health, necessitating advanced remediation strategies. Nanotechnology, leveraging the unique physicochemical properties of materials at the…
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Artikel Jurnal
On-site therapeutic drug analysis with paper-capillary spray ionization and miniature mass spectrometry system
Therapeutic drug monitoring ensures safe and effective pharmacotherapy by maintaining drug concentrations within a therapeutic range. However, conventional liquid chromatography-mass spectrometry workflows are restricted to clinical laboratories and limited by complicated sample preparation and…
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Artikel Jurnal
Environmental fingerprinting of recent strategies for detection of macrolides and fluoroquinolones in environmental and food matrices based on green analytical chemistry indexes
Antibiotic resistance is a growing issue around the world, with an increasing number of diseases becoming more challenging to treat due to the decreasing effectiveness of antibiotics. One approach to controlling this problem is through adequate usage and disposal of antibiotics. Monitoring their…
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Artikel Jurnal
Automated solid phase extraction combined with gas chromatography-mass spectrometry methods for plastic and tire additives in surface waters: development, validation and greenness assessment
Automated solid phase extraction (SPE) combined with gas chromatography-mass spectrometry (GC–MS) methods were proposed for determination of plastic and tire additives in surface water. The plastic additives studied were phthalates (PAEs) and bisphenols (BPs), and the tire additives were…
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Artikel Jurnal
A green GC/FID engineering control to prevent carcinogenic exposure and chemical waste in petrochemical aldehyde monitoring
Chronic occupational exposure to styrene monomer (SM), a Group 2B carcinogen per IARC, represents a critical environmental and public health concern in petrochemical industries, particularly during routine aldehyde monitoring that requires direct handling of raw SM and toxic reagents (methanol…
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Artikel Jurnal
Rapid and high-throughput analysis of PAHs and pesticides adsorbed on microplastics using SPME-MS through a microfluidic open interface coupled to liquid electron ionization mass spectrometry
Microplastics (MPs) are pervasive contaminants in aquatic environments, capable of adsorbing and transporting hazardous chemicals such as polycyclic aromatic hydrocarbons (PAHs) and pesticides. Understanding these adsorption processes is crucial for evaluating their ecological and health risks. In…
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Artikel Jurnal
Can artificial intelligence assist experts in evaluating new analytical methodologies? Stop-flow MicroScale Thermophoresis assessed using the RGB model and AI-Delphi framework
Stop-Flow MicroScale Thermophoresis (SF-MST) enables thermophoretic analysis of highly miniaturized samples introduced into ultrathin capillaries by pressure or electrophoresis. Although successfully applied by our group in several research areas, the broader analytical potential and overall added…
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Artikel Jurnal
Sustainable electrochemical biosensor using polyol-protected probes and magnetic MOFs for thermally robust coronavirus gene detection
Magnetic metal–organic frameworks (MMOFs) offer a promising, environmentally conscious platform for electrochemical sensing due to their high surface area, easy functionalization, and compatibility with green synthesis routes. In this study, MMOFs were synthesized using ferric chloride, imidazole…
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Artikel Jurnal
Determination of flavor compounds sorbed by packaging materials using the purge and trap method
Flavor sorption in food packaging, known as flavor scalping, is a common problem that has a significant impact on the quality of the contents. Flavor sorption by packaging materials is generally measured using the liquid extraction method, which is very time-consuming, laborious, and uses organic…